Vol. 5, Issue 1 (2017)
Synthesis and characterization of biologically active N2O2 type of Novel Schiff base metal complexes derived from 4-amino antipyrine using TEA
Author(s): Sharad D Dakore, VT Kamble and Parshuram Pisal
Abstract: New Schiff base complexes of Cu (II), Co (II), Ni (II) and Zn (II) have been synthesized. Schiff bases synthesized from 4-amino antipyrine, 2- furan carboxaldehyde & acetyl acetone in first step. In second step metal complexes are prepared from synthesized schiff base and divalent metal ions. In both the steps silica supported tri ethylamine catalyst is used at room temperature. The complexes were characterized by IR, 1H NMR, EPR spectro, magnetic moments, conductance, thermal analysis (TGA & DTA), and powder x-ray analysis (XRD). The antimicrobial studies of these complexes against staphylococcus typhi, staphylococcus aureus, Escherichia coli, Bacillus subtilis species by minimum inhibitory consent ratio (MIC) method revealed that these complexes possess potent antibacterial activity.
Pages: 110-113 | 1726 Views 197 Downloads
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How to cite this article:
Sharad D Dakore, VT Kamble, Parshuram Pisal. Synthesis and characterization of biologically active N2O2 type of Novel Schiff base metal complexes derived from 4-amino antipyrine using TEA. Int J Chem Stud 2017;5(1):110-113.
